Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2486-69-3 → 4-((tert-Butoxycarbonyl)amino)-3-methoxybenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2486-69-3 | HCID 288057 | — |
| 반응물 | 4-{[(Tert-butoxy)carbonyl]amino}benzoic acid | HCID 2755931 | — |
| 생성물 | 4-((tert-Butoxycarbonyl)amino)-3-methoxybenzoic acid | HCID 15432033 | — |
반응 단계
4-Amino-3-methoxybenzoic acid (1 g, 5.98 mmol) was reacted according to the same procedure as that used in the process for preparing N-BOC-4-aminobenzoic acid. The resulting solid was recrystallized from ethyl acetate and hexanes to provide the desired product (1.5 g) as tan crystals: m.p. 176-178° C.;
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06310095B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-36157f54cbef4f0698d56bb9a849c58e |
| 출처 메모 | uspto-grants-2001_10 |