Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → (2-Acetyl-4-methylpentyl)trimethylammonium Iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 3-((Dimethylamino)methyl)-5-methyl-2-hexanone | HCID 53419039 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | (2-Acetyl-4-methylpentyl)trimethylammonium Iodide | HCID 86641883 | 68.4% |
반응 단계
Iodomethane (20 g, 140.94 mmol, 2.00 equiv) was added dropwise to a solution of 3-((dimethylamino)methyl)-5-methylhexan-2-one (12 g, 70.05 mmol, 1.00 equiv) and ethyl acetate (50 mL). The solution was stirred at ambient temperature for about 16 hours., and the resulting preciptant was collected by filtration to afford the title product (15 g, yield=68%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524733B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-279e4411a2944fb7abb24634632e5481 |
| 출처 메모 | uspto-grants-2013_09 |