Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclohexyl isocyanate → HCID 178418497, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclohexyl isocyanate | HCID 18502 | — |
| 반응물 | 3-[4-(4-Chlorophenethyl)piperazin-1-yl]propanethiol | HCID 13731125 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178418497 | HCID 178418497 | 170.7% |
반응 단계
The procedure described in Example 35 was followed, using 1.7 g of cyclohexyl isocyanate, 4.0 g of 3-[4-(4-chlorophenethyl)piperazin-1-yl]propanethiol and 100 ml of methylene chloride, to give 3.8 g (58% of theory) of N-cyclohexyl-S-{3-[4-(4-chlorophenethyl)piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 262°-267° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04722926 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-a34cebc025d14918a8b53e7fb7577a4a |
| 출처 메모 | uspto-grants-1988_02 |