Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → HCID 178418568, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Hexyl isocyanate | HCID 75659 | — |
| 반응물 | 3-(4-Cinnamylpiperazin-1-yl)propanethiol dihydrochloride | HCID 73186836 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178418568 | HCID 178418568 | 64.2% |
반응 단계
The procedure described in Example 2 was followed, using 0.4 g of n-hexyl isocyanate, 1.0 g of 3-(4-cinnamylpiperazin-1-yl)propanethiol dihydrochloride, 0.6 g of triethylamine and 50 ml of methylene chloride, to give 0.44 g (31% of theory) of N-(n-hexyl)-S-[3-(4-cinnamylpiperazin-1-yl)propyl]thiocarbamate dihydrochloride as a white crystalline solid, M.p. 251°-253° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04722926 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-ed77c6d5e9bf4296bf37b6996aa0f6d8 |
| 출처 메모 | uspto-grants-1988_02 |