Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 384574생성일: 2026년 10월 25일
2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate → HCID 178441701, 화합물
https://huagongshe.com/reaction/384574
참여 물질
| 역할 | 이름 | HCID | 투입량 |
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| 반응물 | 2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate | HCID 67979259 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | HCID 178441701 | HCID 178441701 | — |
반응 단계
2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2′-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate (1130 mg, 1.48 mmol) was dissolved in concentrated hydrochloric acid (24 mL). The solution was stirred at 100° C. for 30 minutes. The solution was washed with diethyl ether (2×) and the aqueous layer was concentrated in vacuo. The residue was used crude in the following step. LC-MS: m/z 495.0 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08367711B2 |
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| 출처 데이터셋 | uspto-grants-2013_02 |
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| ORD ID | ord-15a211b0ad824bbc8bada56abf249e52 |
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| 출처 메모 | uspto-grants-2013_02 |
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