Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 1-Bromo-2-fluoro-4-(2,2,3,3,3-pentafluoro-propoxy)-benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2,2,3,3,3-Pentafluoropropyl trifluoromethanesulfonate | HCID 2776019 | — |
| 반응물 | 4-Bromo-3-fluorophenol | HCID 2779153 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 1-Bromo-2-fluoro-4-(2,2,3,3,3-pentafluoro-propoxy)-benzene | HCID 87443298 | — |
반응 단계
The title compound was prepared from 4-bromo-3-fluorophenol and 2,2,3,3,3,-pentafluoropropyl triflate with potassium carbonate in acetone at ambient temperature for 18 hours. Kugelrohr distillation provided a colorless oil, b.p. 105-110° C./12 mbar.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08367838B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-7ef815b8595f4da1b115d094560517b9 |
| 출처 메모 | uspto-grants-2013_02 |