Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Rac-1-bromo-4-(2,2,2-trifluoro-1-methyl-ethoxy)-benzene → Rac-[1-(4-chloro-phenyl)-2-oxo-2-[4-(2,2,2-trifluoro-1-methyl-ethoxy)-phenyl]-ethyl]-carbamic acid tert-butyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Rac-1-bromo-4-(2,2,2-trifluoro-1-methyl-ethoxy)-benzene | HCID 68408561 | — |
| 반응물 | Rac-[(4-chloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester | HCID 71663866 | — |
| 생성물 | Rac-[1-(4-chloro-phenyl)-2-oxo-2-[4-(2,2,2-trifluoro-1-methyl-ethoxy)-phenyl]-ethyl]-carbamic acid tert-butyl ester | HCID 68409760 | — |
반응 단계
The title compound was prepared from rac-[(4-chloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester (Intermediate 8) and rac-1-bromo-4-(2,2,2-trifluoro-1-methyl-ethoxy)-benzene (Intermediate 35) in analogy to Example 1a): MS (ISP): 458.2 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08367838B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-a339dd7dc2b946d989b6a0154580aafc |
| 출처 메모 | uspto-grants-2013_02 |