참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-Cyano-4-methoxybenzoic acid | HCID 21990972 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 3-Cyano-4-methoxybenzoyl chloride | HCID 20254941 | — |
반응 단계
To 3-cyano-4-methoxybenzoic acid (1.78 g), toluene (20 mL), N,N-dimethylformamide (3 droplets) and thionyl chloride (1.14 mL) were added, and then the mixture was stirred at 60° C. for 16 hours. The solvent was distilled off under reduced pressure and the obtained residue was azeotroped with toluene and used for the synthesis of (d).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08367843B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_02 |
|---|
| ORD ID | ord-ddd393383c0b4ed59530ffcd6f1c55e5 |
|---|
| 출처 메모 | uspto-grants-2013_02 |
|---|
