Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodine → Muconic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodine | HCID 807 | — |
| 반응물 | (2E,4Z)-2,4-Hexadienedioic acid | HCID 5280614 | — |
| 용매 | 1-Propanol | HCID 1031 | — |
| 생성물 | Muconic Acid | HCID 5356793 | 73% |
반응 단계
cis,trans-Muconic acid (103 mg, 0.725 mmol) is dissolved in n-propanol (10 mL) at room temperature and a crystal of iodine (10 mg, 0.04 mmol) is added. The reaction mixture is allowed to stir at room temperature for 24 hours. The precipitate is filtered, washed with acetonitrile and dried under reduced pressure to yield 75 mg of trans,trans-muconic acid, a 73 percent yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08367858B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-43b6087262e946d986e929fdc93548e2 |
| 출처 메모 | uspto-grants-2013_02 |