Thionyl Chloride → HCID 59526066, 화합물

HRID 386120노트

반응식

HRID 386120 반응식
[CH3:1][C:2](=[N:4][O:5][CH2:6][C:7]([OH:9])=O)[CH3:3].S(Cl)([Cl:12])=O>C1(C)C=CC=CC=1>[CH3:1][C:2](=[N:4][O:5][CH2:6][C:7]([Cl:12])=[O:9])[CH3:3]

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 79344[(2-Propanylideneamino)oxy]acetic acid

생성물 1

HCID 59526066HCID 59526066, 화합물

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

To {[(1-methylethylidene)amino]oxy}acetic acid (286 g, 2.18 mol) was added 600 ml of toluene. Thionyl chloride (364 g, 3.06 mol) was added dropwise at room temperature. After the addition was complete, the reaction mixture was heated to reflux for 10 hours. Toluene and thionyl chloride were evaporated under vacuum and the residue was distilled to afford the title compound.

후처리

  1. additionAfter the addition
  2. temperaturethe reaction mixture was heated
  3. temperatureto reflux for 10 hours
  4. customToluene and thionyl chloride were evaporated under vacuum
  5. distillationthe residue was distilled

출처 및 근거

ORD 기록
ord-10e3dbd5cef642c3a68a50a65e46166f
출처 데이터셋
uspto-grants-2013_02
특허 번호
US08367706B2

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