HCID 135736201, 화합물 → 8-(2-Dimethylamino-4-nitro-phenyl)purin-6-one

HRID 3863노트

반응식

HRID 3863 반응식
[NH2:1][C:2]1[C:7](=[O:8])[NH:6][CH:5]=[N:4][C:3]=1[NH:9][C:10](=O)[C:11]1[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][C:12]=1[N:20]([CH3:22])[CH3:21]>C(O)(=O)C>[CH3:21][N:20]([CH3:22])[C:12]1[CH:13]=[C:14]([N+:17]([O-:19])=[O:18])[CH:15]=[CH:16][C:11]=1[C:10]1[N:1]=[C:2]2[C:3](=[N:4][CH:5]=[N:6][C:7]2=[O:8])[N:9]=1

참가 물질

3

반응물 1

HCID 135736201HCID 135736201, 화합물

생성물 1

HCID 201532228-(2-Dimethylamino-4-nitro-phenyl)purin-6-one

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

One gram of 5-amino-4-(2-dimethylamino-4-nitro-benzoylamino)pyrimidin-6-one is refluxed for two hours in 50 ml of glacial acetic acid. The mixture is evaporated to dryness, and the residue is stirred out with ethanol in the warm.

후처리

  1. customThe mixture is evaporated to dryness

출처 및 근거

ORD 기록
ord-cd16ce517d74444e9c3738b0eac46728
출처 데이터셋
uspto-grants-1988_02
특허 번호
US04722929

반응 노트

불러오는 중…