참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2-Propenoic acid, 3-(4-nitrophenyl)- | HCID 70156 | — |
| 생성물 | Methyl 3-(4-nitrophenyl)-2-propenoate | HCID 5354137 | — |
반응 단계
A solution of p-nitrocinnamic acid (3.86 g, 20.0 mmol) in MeOH (50 mL) was treated with H2SO4 (2 mL) and was stirred at 25° C. for 24 h. Concentration afforded S31 (4.10 g, 19.8 mmol, 99%) as a yellow solid: 1H NMR (CDCl3, 500 MHz) 8.26 (d, 2H, J=8.4 Hz), 7.12 (d, 1H, J=16.1 Hz), 7.68 (d, 2H, J=8.8 Hz), 6.58 (d, 1H, J=16.1 Hz), 3.85 (s, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08372823B2 |
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| 출처 데이터셋 | uspto-grants-2013_02 |
|---|
| ORD ID | ord-2d6371425109489396de1ea2680e66a5 |
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| 출처 메모 | uspto-grants-2013_02 |
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