Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → HCID 57419860, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-Bromo-4-fluorophenylacetic Acid | HCID 3416339 | — |
| 생성물 | HCID 57419860 | HCID 57419860 | — |
반응 단계
3-Bromo-4-fluorophenylacetic acid (2.078 g, 8.92 mmol) and thionyl chloride (1.3 mL, 17.84 mmol) were combined in MeOH (20 mL) and stirred at room temperature for 10 minutes. The mixture was concentrated, and the residue was worked up with CH2Cl2 and 1N aqueous NaOH. The organic layer was dried over MgSO4, filtered, and concentrated to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524748B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-ed4b6c1e36844eacaa4bfe898d5b7ccd |
| 출처 메모 | uspto-grants-2013_09 |