돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 38699생성일: 2026년 10월 25일

Methanol → HCID 57419860, 화합물

https://huagongshe.com/reaction/38699

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물Thionyl ChlorideHCID 24386—
반응물3-Bromo-4-fluorophenylacetic AcidHCID 3416339—
생성물HCID 57419860HCID 57419860—

반응 단계

3-Bromo-4-fluorophenylacetic acid (2.078 g, 8.92 mmol) and thionyl chloride (1.3 mL, 17.84 mmol) were combined in MeOH (20 mL) and stirred at room temperature for 10 minutes. The mixture was concentrated, and the residue was worked up with CH2Cl2 and 1N aqueous NaOH. The organic layer was dried over MgSO4, filtered, and concentrated to give the title compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08524748B2
출처 데이터셋uspto-grants-2013_09
ORD IDord-ed4b6c1e36844eacaa4bfe898d5b7ccd
출처 메모uspto-grants-2013_09