참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 8-(2-Methoxy-4-benzyloxy-phenyl)-2-chloro-purine | HCID 13532386 | — |
| 용매 | Benzyl Alcohol | HCID 244 | — |
| 생성물 | 8-(2-Methoxy-4-benzyloxy-phenyl)-2-benzyloxypurine | HCID 13532399 | — |
반응 단계
An amount of 4.5 gm of powdered potassium hydroxide is dissolved in 70 ml of benzyl alcohol, and then 7.2 gm of 8-(2-methoxy-4-benzyloxy-phenyl)-2-chloro-purine are added. The mixture is heated to 150° C. for three hours, cooled, and filtered, the filtrate is mixed with ether, and the precipitate obtained is purified by chromatography on silica gel [eluant: methylene chloride/ethanol (100:2.5)].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04722929 |
|---|
| 출처 데이터셋 | uspto-grants-1988_02 |
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| ORD ID | ord-18a6059416844248a8ba411c923fd244 |
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| 출처 메모 | uspto-grants-1988_02 |
|---|
