Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroxylamine → (E)-4-bromo-1-naphthaldehyde oxime
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroxylamine | HCID 787 | — |
| 반응물 | 4-Bromo-1-naphthaldehyde | HCID 4640413 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | (E)-4-bromo-1-naphthaldehyde oxime | HCID 74016047 | — |
반응 단계
Hydroxylamine (50% aqueous, 0.37 ml) is added to a solution of 4-bromo-naphthalene-1-carbaldehyde (0.7 g) in methanol (6 ml). After 16 hours at room temperature the reaction is concentrated in vacuo to yield crude 4-bromo-naphthalene-1-carbaldehyde oxime, which is used in the next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08377942B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-2e7b1da0e29743ba91047d2ec95dec3e |
| 출처 메모 | uspto-grants-2013_02 |