Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 2,4-Dimethyl-5-nitroaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | 2,4-Dimethylaniline | HCID 7250 | — |
| 용매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | 2,4-Dimethyl-5-nitroaniline | HCID 228007 | — |
반응 단계
To a mixture of 2,4-dimethylaniline (10 mmol) in 5 mL of conc. H2SO4, fuming HNO3 (90%; 0.6 mL) was added dropwise at 0° C. The resulting mixture was stirred for 12 h at RT and then slowly poured into ice. The solid was collected by filtration and dried to yield 2,4-dimethyl-5-nitroaniline as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08377983B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-38f61b6dd6a747a09f3247a5f0ece124 |
| 출처 메모 | uspto-grants-2013_02 |