참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,4-Dichlorobenzene | HCID 4685 | — |
| 반응물 | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| 반응물 | 1-(Iodomethyl)-3,5-dinitrobenzene | HCID 22609073 | — |
| 생성물 | 1-(3,5-dinitrobenzyl)-2,3,3-trimethyl-3H-indolium iodide | HCID 17902140 | 55.9% |
반응 단계
To 2,3,3-trimethylindolenine (1.64 g) was added 3,5-dinitrobenzyl iodide (3.71 g) and dichlorobenzene (15 ml). After heating to 90° C. for 6 hours the mixture was allowed to cool and the resultant precipitate removed by filtration. The solid was washed with dichlorobenzene (2×10 ml) and ether (2×50 ml). The material was dried in a vacuum oven to give the product as a yellow solid (2.69 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08378120B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_02 |
|---|
| ORD ID | ord-754140fff8a546979a083679d9b20aac |
|---|
| 출처 메모 | uspto-grants-2013_02 |
|---|
