참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,4-Dichlorobenzene | HCID 4685 | — |
| 반응물 | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| 반응물 | 1-Bromo-3,6-dioxaheptane | HCID 123532 | — |
| 생성물 | 1-(2-(2-Methoxyethoxy)ethyl)-2,3,3-trimethyl-3h-indolium bromide | HCID 68813660 | — |
반응 단계
To 2,3,3-trimethylindolenine (1.59 g) was added 1-bromo-2-(2-methoxyethoxy)ethane (2.75 g) and dichlorobenzene (5 ml). The mixture was heated to 70° C. overnight. The volatiles were stripped and the material purified by HPLC.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08378120B2 |
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| 출처 데이터셋 | uspto-grants-2013_02 |
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| ORD ID | ord-d7d322c6a96a4247a8c483bed3a38135 |
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| 출처 메모 | uspto-grants-2013_02 |
|---|