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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 389236생성일: 2026년 10월 25일

1,4-Dichlorobenzene → 1-(2-(2-Methoxyethoxy)ethyl)-2,3,3-trimethyl-3h-indolium bromide

https://huagongshe.com/reaction/389236

반응식

참여 물질

역할이름HCID투입량
반응물1,4-DichlorobenzeneHCID 4685—
반응물3H-Indole, 2,3,3-trimethyl-HCID 15427—
반응물1-Bromo-3,6-dioxaheptaneHCID 123532—
생성물1-(2-(2-Methoxyethoxy)ethyl)-2,3,3-trimethyl-3h-indolium bromideHCID 68813660—

반응 조건

온도70 °C

반응 단계

To 2,3,3-trimethylindolenine (1.59 g) was added 1-bromo-2-(2-methoxyethoxy)ethane (2.75 g) and dichlorobenzene (5 ml). The mixture was heated to 70° C. overnight. The volatiles were stripped and the material purified by HPLC.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08378120B2
출처 데이터셋uspto-grants-2013_02
ORD IDord-d7d322c6a96a4247a8c483bed3a38135
출처 메모uspto-grants-2013_02