참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-Methyl-2-butanone | HCID 11251 | — |
| 반응물 | 4-Methoxyphenylhydrazine hydrochloride | HCID 2723904 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 5-Methoxy-2,3,3-trimethyl-3H-indole | HCID 11095392 | — |
반응 단계
To 4-methoxyphenyl hydrazine hydrochloride (4.84 g) was added 3-methyl-2-butanone (6.4 ml) and acetic acid (45 ml). The mixture was heated to 10° C. for 2.5 hours after which time the solvent was removed by rotary evaporation. Flash column chromatography gave the product (4.66 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08378120B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_02 |
|---|
| ORD ID | ord-0f58494c1ef14cdc90d2e0dcd78b2684 |
|---|
| 출처 메모 | uspto-grants-2013_02 |
|---|
