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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 389240생성일: 2026년 10월 26일

Iodoethane → 3H-Indolium, 1-ethyl-5-methoxy-2,3,3-trimethyl-, iodide

https://huagongshe.com/reaction/389240

반응식

참여 물질

역할이름HCID투입량
반응물IodoethaneHCID 6340—
반응물5-Methoxy-2,3,3-trimethyl-3H-indoleHCID 11095392—
용매1,2-DichlorobenzeneHCID 7239—
생성물3H-Indolium, 1-ethyl-5-methoxy-2,3,3-trimethyl-, iodideHCID 10427640—

반응 조건

온도80 °C

반응 단계

To 5-methoxy-2,3,3-trimethyl-3H-indole (1.9 g) was added iodoethane (5 ml) and 1,2-dichlorobenzene (10 ml). The mixture was heated to 80° C. for 4 hours after which time the mixture was allowed to cool and the precipitate removed by filtration and washed sequentially with dichlorobenzene and diethyl ether. Drying in a vacuum oven gave the product (3 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08378120B2
출처 데이터셋uspto-grants-2013_02
ORD IDord-1ad63baa8ad949f5b011d549a550d294
출처 메모uspto-grants-2013_02