Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 38926생성일: 2026년 10월 25일
Allylamine → N-{[5-Fluoro-7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-YL]methyl}prop-2-EN-1-amine
https://huagongshe.com/reaction/38926
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Allylamine | HCID 7853 | — |
| 반응물 | [5-Fluoro-7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-yl]methyl 4-methylbenzenesulfonate | HCID 86652936 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-{[5-Fluoro-7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-YL]methyl}prop-2-EN-1-amine | HCID 44469878 | — |
반응 단계
A mixture of [5-fluoro-7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-yl]methyl-4-methylbenzenesulfonate (0.005 g, 0.012 mmol), prop-2-en-1-amine (0.5 ml) and ACN (2.5 ml) was heated under microwave radiation at 120° C. for 20 min. MS m/z (rel. intensity, 70 eV) 301 (M+, 2), 71 (5) 70 (bp), 69 (4) 68 (5).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08524766B2 |
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| 출처 데이터셋 | uspto-grants-2013_09 |
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| ORD ID | ord-42477169d453425ca2e247d102ddb151 |
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| 출처 메모 | uspto-grants-2013_09 |
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