Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonic acid → 1-Acetoxy-3-(8,11,14-pentadecatrienyl) benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Cardanol | HCID 11266523 | — |
| 생성물 | 1-Acetoxy-3-(8,11,14-pentadecatrienyl) benzene | HCID 69049096 | — |
반응 단계
A mixture of acetic anhydride (0.1 mol, 15 ml) and p-toluenesulphonic acid (PTSA, 3.15 mol %, 0.6 g) were taken in a two necked RB flask and double distilled cardanol (0.1 mol, 30 g) was added dropwise with stirring over a period of 30 minutes at ambient conditions. The reaction was continued for 8-12 h. The product (AC) was washed free of acetic acid and catalyst with water and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08378135B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-eef7ad41575b4ffdbb03c5667438d682 |
| 출처 메모 | uspto-grants-2013_02 |