Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Propanamine, N-ethyl- → N-Ethyl-N-{[7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}propan-1-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Propanamine, N-ethyl- | HCID 88398 | — |
| 반응물 | [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate | HCID 86652940 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-Ethyl-N-{[7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}propan-1-amine | HCID 44468512 | — |
반응 단계
Preparation according to Example 25: [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate (0.020 g, 0.0504 mmol), N-ethylpropan-1-amine (0.5 ml), ACN (3 ml). MS m/z (rel. intensity, 70 eV) 311 (M+, 1), 282 (5), 101 (8), 100 (bp), 72 (6), 58 (9).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524766B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-ca59e52c68d74e00b761c37003e3cb1f |
| 출처 메모 | uspto-grants-2013_09 |