Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Methylethylamine → N-Methyl-N-{[7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}ethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Methylethylamine | HCID 12219 | — |
| 반응물 | 2,2-Dimethyl-N-{[(2S)-7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-YL]methyl}propan-1-amine | HCID 44468378 | — |
| 반응물 | [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate | HCID 86652940 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-Methyl-N-{[7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}ethanamine | HCID 44468652 | — |
반응 단계
Preparation according to Example 25: [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate (0.020 g, 0.0504 mmol), N-methylethanamine (0.5 ml), ACN (3 ml). MS m/z (rel. intensity, 70 eV) 283 (M+, 2), 131 (4), 77 (4), 73 (5), 72 (bp), 63 (2).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524766B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-c71b1b288cd343e089c69a7a28d1386f |
| 출처 메모 | uspto-grants-2013_09 |