Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 2-Hydroxy-1-(3-methylphenyl)ethan-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 2-Bromo-1-(3-methylphenyl)ethan-1-one | HCID 10036129 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 2-Hydroxy-1-(3-methylphenyl)ethan-1-one | HCID 18372905 | — |
반응 단계
A solution of 2-bromo-1-(3-methylphenyl)ethanone (1 g) in acetonitrile (2.5 mL) and water (13 mL) is treated under microwave irradiation (125° C., 50 min). The same experiment is repeated three times. All the vials are collected, extracted with DCM, dried over magnesium sulfate and concentrated under vacuum to give the desired compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08383608B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-53b1fb3a11334045a8e1fdc82626b016 |
| 출처 메모 | uspto-grants-2013_02 |