Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → (NZ)-N-[3-(4-chlorophenyl)-1,3-thiazolidin-2-ylidene]-3-methylimidazol-3-ium-1-carboxamide iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | HCID 87449094 | HCID 87449094 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | (NZ)-N-[3-(4-chlorophenyl)-1,3-thiazolidin-2-ylidene]-3-methylimidazol-3-ium-1-carboxamide iodide | HCID 87447829 | — |
반응 단계
N-[(2Z)-3-(4-Chlorophenyl)-1,3-thiazolidin-2-ylidene]-1H-imidazole-1-carboxamide (320 mg, 1.043 mmol, Example 25A) was suspended in dry acetonitrile (5 mL), and then iodomethane (0.325 mL, 5.22 mmol) was added. The mixture stirred at room temperature. After four days, the solvent was evaporated to give the title product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08383657B2 |
| 출처 데이터셋 | uspto-grants-2013_02 |
| ORD ID | ord-9fa71b9d1bd841759cde32862025345d |
| 출처 메모 | uspto-grants-2013_02 |