Ethyl 3-hydroxybenzoate → 3-(Tetrahydropyran-4-yloxy)benzoic acid

반응식

[OH:1][CH:2]1[CH2:7][CH2:6][O:5][CH2:4][CH2:3]1.O[C:9]1[CH:10]=[C:11]([CH:17]=[CH:18][CH:19]=1)[C:12]([O:14]CC)=[O:13]>>[O:5]1[CH2:6][CH2:7][CH:2]([O:1][C:9]2[CH:10]=[C:11]([CH:17]=[CH:18][CH:19]=2)[C:12]([OH:14])=[O:13])[CH2:3][CH2:4]1

참가 물질

반응물 2

HCID 24522Ethyl 3-hydroxybenzoate

HCID 74956Tetrahydro-4H-pyran-4-ol

생성물 1

HCID 231490603-(Tetrahydropyran-4-yloxy)benzoic acid

실험 절차

Prepared from 4-hydroxy-tetrahydropyrane and ethyl 3-hydroxybenzoate. LC-MS (m/z): 245 (M−23 (Na)).

출처 및 근거

ORD 기록: ord-d298da15c63c40849bc6ffbfe1de02de
출처 데이터셋: uspto-grants-2013_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08383820B2

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