참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methacrylic Acid | HCID 4093 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Silane, (chloromethyl)trimethyl- | HCID 75361 | — |
| 용매 | Dimethylazanide | HCID 182180 | — |
| 생성물 | Methacryloxymethyltrimethylsilane | HCID 2760855 | — |
반응 단계
300 mmol of Methylacrylic acid (MAA) and 200 mmol of chloromethyl trimethylsilane were dissolved in 400 ml of dimethylamide. Potassium carbonate was added to the solution and heated to 90° C. and stirred for 5 hours. Next, the reaction solution was filtered. The filtrate was added to a sodium hydrogen carbonate solution, extracted with ether and pure water respectively, dried, filtered, and concentrated to obtain trimethylsilanylmethyl methylacrylate (TMSA) having the formula (i) below
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06800420B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_10 |
|---|
| ORD ID | ord-89374aab0d65459ebc755dc684689d3d |
|---|
| 출처 메모 | uspto-grants-2004_10 |
|---|
