Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 392011생성일: 2026년 10월 24일
Dicyclopentadiene → 8-(2,2,2-Trifluoro-1-trifluoromethyl-1-hydroxyethyl)tetracyclo[4.4.0.12,5.17,10]dodec-3-ene
https://huagongshe.com/ko/reaction/392011
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dicyclopentadiene | HCID 6492 | — |
| 반응물 | 4-Penten-2-ol, 1,1,1-trifluoro-2-(trifluoromethyl)- | HCID 328870 | — |
| 생성물 | 8-(2,2,2-Trifluoro-1-trifluoromethyl-1-hydroxyethyl)tetracyclo[4.4.0.12,5.17,10]dodec-3-ene | HCID 20617087 | 22.2% |
반응 단계
A 500 ml autoclave was charged with 230 g of 1,1-bis(trifluoromethyl)-3-butenol, 73 g of dicyclopentadiene, and 0.15 g of 2,6-di-t-butylparacresol, and the mixture was heated at 190° C. for 12 hours. The reaction solution was cooled to room temperature and purified by distillation to obtain 40 g of 8-(2,2,2-trifluoro-1-trifluoromethyl-1-hydroxyethyl)tetracyclo[4.4.0.12,5.17,10]dodec-3-ene of the following formula (13).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06800414B2 |
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| 출처 데이터셋 | uspto-grants-2004_10 |
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| ORD ID | ord-c5a8c281d9034da7adddb676a06667da |
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| 출처 메모 | uspto-grants-2004_10 |
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