Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperidine → Phe-Gly
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | Fmoc-Phe-Gly-OH | HCID 11328236 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Phe-Gly | HCID 6992304 | — |
반응 단계
Fmoc-protected dipeptide 72 (500 mg, 1.00 mmol) was treated with a 5% v/v solution of piperidine in DMF (5 mL). After stirring for 1 h, the reaction mixture was concentrated to dryness. The crude material was used for the next step without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524691B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-f2ae1b8090a940d2913985de4b8df854 |
| 출처 메모 | uspto-grants-2013_09 |