참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triethoxychlorosilane | HCID 78398 | — |
| 반응물 | Sodium chlorodifluoroacetate | HCID 2734985 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Chlorodifluoroacetic acid, triethoxysilyl ester | HCID 23523584 | — |
반응 단계
15.246 g (0.10 mol) sodium chlorodifluoroacetate, is dissolved to 100 mL Et2O and cooled to −70° C. 19.7 mL (0.10 mol, 19.872 g) chlorotriethoxysilane in Et2O (50 mL) was added dropwise to reaction solution. The solution was stirred for over night allowing it to warm up to room temperature. NaCl is removed by filtration and solution evaporated to dryness to result clear colourless liquid, chlorodifluoroacetic acid, triethoxysilyl ester.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06803476B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_10 |
|---|
| ORD ID | ord-952c4637cec247c382f31cb28c094e32 |
|---|
| 출처 메모 | uspto-grants-2004_10 |
|---|
