Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N,3-trimethyl-4-nitrobenzamide → 4-amino-N,N,3-trimethylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N,3-trimethyl-4-nitrobenzamide | HCID 786992 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-amino-N,N,3-trimethylbenzamide | HCID 16781770 | — |
반응 단계
N,N,3-trimethyl-4-nitrobenzamide (0.6 g, 2.88 mmol) in methanol was hydrogenated using the H-cube apparatus (1.2 mL/min, RT, atmospheric pressure). After 45 minutes the reaction was complete. Removal of the solvent in vacuo gave 4-amino-N,N,3-trimethylbenzamide as a colourless solid (quantitative); MS (ES+) 179.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524902B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-3fa264f9a8bd4375af3bdd364a61e69a |
| 출처 메모 | uspto-grants-2013_09 |