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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 393492생성일: 2026년 10월 24일

1-O-alpha-D-Glucopyranosyl-D-mannitol → Trehalose

https://huagongshe.com/ko/reaction/393492

반응식

참여 물질

역할이름HCID투입량
반응물1-O-alpha-D-Glucopyranosyl-D-mannitolHCID 88735—
용매WaterHCID 962—
생성물TrehaloseHCID 7427—

반응 조건

온도125 °C

반응 단계

Ninety-five parts by weight of high-purity crystalline trehalose hydrate and 18 parts by weight of palatinit were placed in a dissolving tank, and admixed with and dissolved by heating in 63 parts by weight of water. The solution was placed in a concentrator, concentrated to boil down by heating to 125° C. under reduced pressure, continued concentrating by heating under reduced pressure while keeping the temperature until reaching to a moisture content of about 1.0%. Similarly as in Example A-1, the concentrate was subjected to an extruder for forming, cooled to ambient temperature to obtain a short-rod thermoplastic shaped-body of trehalose, about 2 mm in diameter and about 4 mm in length. Since the product was a colorless, transparent or translucent, and substantially amorphous shaped-body having thermoplasticity and satisfactory storage-stability under indoor circumstances, it can be arbitrarily reheated to a temperature of about 90° C. to about 160° C. to impart it free-flowing ability, then transformed or processed into a shaped-body with an appropriate form with or without using other substances having different functions. The product can be also used arbitrarily for preparing a paste containing trehalose by dissolving in a relatively-small amount of hot water, and the resulting paste can be used intact in an amorphous form or used as a powdered base after crystallization of trehalose.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06808651B1
출처 데이터셋uspto-grants-2004_10
ORD IDord-e2d0f268a5e4473baed019330ac142fc
출처 메모uspto-grants-2004_10