Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,6-Hexanediol → 5,7-di-tert-butyl-3-(4-n-octyloxycarbonylphenyl)-3H-benzofuran-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,6-Hexanediol | HCID 12374 | — |
| 반응물 | 1,12-Dodecanediol | HCID 79758 | — |
| 반응물 | 5,7-di-tert-butyl-3-(4-methoxycarbonylphenyl)-3H-benzofuran-2-one | HCID 12162160 | — |
| 생성물 | 5,7-di-tert-butyl-3-(4-n-octyloxycarbonylphenyl)-3H-benzofuran-2-one | HCID 22648338 | — |
반응 단계
Compounds (111), (112), (113), (114), (115), (116) and (117) (Table 1) are obtained in analogy to Example 5 using 1-dodecanol, 1-octadecanol, 1-nonadecanol, 1-docosanol, 2-ethylhexanol, 1,6-hexanediol and 1,12-dodecanediol instead of 1-octanol. For the preparation of compounds (116) and (117) only half of an equivalent of 1,6-hexanediol and 1,12-dodecanediol in respect to the compound (109) was used.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06809208B2 |
| 출처 데이터셋 | uspto-grants-2004_10 |
| ORD ID | ord-4c4698c17a3644e8b1679f03c35a3398 |
| 출처 메모 | uspto-grants-2004_10 |