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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 3949생성일: 2026년 10월 23일

2,3,3,3-Tetrafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)propanoyl fluoride → Sodium 2,3,3,3-tetrafluoro-2-(heptafluoropropoxy)propanoate

https://huagongshe.com/ko/reaction/3949

반응식

참여 물질

역할이름HCID투입량
반응물2,3,3,3-Tetrafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)propanoyl fluorideHCID 102740—
반응물Sodium trimethylsilanolateHCID 23672319—
용매TetrahydrofuranHCID 8028—
생성물Sodium 2,3,3,3-tetrafluoro-2-(heptafluoropropoxy)propanoateHCID 376511869.3%

반응 단계

The procedure of Example 1 was followed using perfluoro-2-methyl-3-oxahexanoyl fluoride (16.6 g, 50 mmol), sodium trimethylsilanolate (5.6 g, 50 mmol), and dry tetrahydrofuran (100 mL), and a 2 h reaction time. Sodium perfluoro-2-methyl-3-oxahexanoate (12.2 g, 69% yield) was isolated as a white solid: The 19F NMR data were the same as reported in Example 15.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04723016
출처 데이터셋uspto-grants-1988_02
ORD IDord-a2d4c15aa91b4bc49e43d3bde49780ee
출처 메모uspto-grants-1988_02