Potassium Carbonate → HCID 22568938, 화합물

HRID 395144노트

반응식

HRID 395144 반응식
[CH2:1]([O:3][C:4]1([C:7]2[CH:12]=[CH:11][C:10]([C:13]#[C:14][Si](C)(C)C)=[CH:9][C:8]=2[CH:19]([CH3:21])[CH3:20])[CH2:6][CH2:5]1)[CH3:2].C(=O)([O-])[O-].[K+].[K+]>CO>[CH2:1]([O:3][C:4]1([C:7]2[CH:12]=[CH:11][C:10]([C:13]#[CH:14])=[CH:9][C:8]=2[CH:19]([CH3:20])[CH3:21])[CH2:6][CH2:5]1)[CH3:2]

참가 물질

4

반응물 2

HCID 11430Potassium CarbonateHCID 22569012[4-(1-Ethoxycyclopropyl)-3-isopropyl-phenylethynyl]-trimethylsilane2회

생성물 1

HCID 22568938HCID 22568938, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Using General Procedure E; [4-(1-ethoxycyclopropyl)-3-isopropyl-phenylethynyl]-trimethylsilane (Intermediate 102,210.0 mg, 0.70 mmol) in methanol (10 mL) was treated with potassium carbonate (100.0 mg, 0.72 mmol) and stirred overnight at ambient temperature. The crude alkyne was used directly in the next reaction.

출처 및 근거

ORD 기록
ord-240c9fd27759471cbf877e35ec518e85
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06603019B2

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