Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Octyltrichlorosilane → Octyltriacetoxysilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Octyltrichlorosilane | HCID 21354 | — |
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 용매 | Heptane | HCID 8900 | — |
| 생성물 | Octyltriacetoxysilane | HCID 13977504 | 88% |
반응 단계
In a 1-1 round-bottomed flask were placed first 55 g of anhydrous sodium acetate, and then 500 ml of anhydrous heptane. To the white suspension formed was added 50 g of octyltrichlorosilane. The reaction medium was left under stirring at ambient temperature for 2 h, and then filtered under argon to remove the precipitate. The filtrate was concentrated to eliminate the heptane, giving 54 g (88% yield) of octyltriacetoxysilane as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06605423B2 |
| 출처 데이터셋 | uspto-grants-2003_08 |
| ORD ID | ord-4ac068724ab44b20bce208aa01a6c954 |
| 출처 메모 | uspto-grants-2003_08 |