(4-Chlorophenyl)hydrazine → HCID 9857479, 화합물

반응식

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8]N)=[CH:4][CH:3]=1.O=[C:11]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[CH2:12][CH2:13][CH2:14][C:15]([O:17]CC)=[O:16]>>[Cl:1][C:2]1[CH:7]=[C:6]2[C:5](=[CH:4][CH:3]=1)[NH:8][C:11]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)=[C:12]2[CH2:13][CH2:14][C:15]([OH:17])=[O:16]

참가 물질

반응물 2

HCID 70624(4-Chlorophenyl)hydrazine

HCID 4164781Ethyl 5-oxo-5-phenylpentanoate

생성물 1

HCID 9857479HCID 9857479, 화합물수율 11%

실험 절차

The expected acid is obtained in the form of a white solid with a yield of 11% by following a procedure analogous to Example 1 and starting from 4-chlorophenylhydrazine and ethyl δ-oxobenzenepentanoate.

출처 및 근거

ORD 기록: ord-34423c9c1cb74d08b82205f417d97da1
출처 데이터셋: uspto-grants-2003_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06605633B1

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