2-Chloro-4-hydroxybenzaldehyde → HCID 21352696, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:26]=[CH:25][C:6]([C:7]([NH:9][C:10]2[C:11]([NH:16][C:17]([CH:19]3[CH2:24][CH2:23][NH:22][CH2:21][CH2:20]3)=[O:18])=[CH:12][CH:13]=[CH:14][CH:15]=2)=[O:8])=[CH:5][CH:4]=1.[Cl:27][C:28]1[CH:35]=[C:34]([OH:36])[CH:33]=[CH:32][C:29]=1[CH:30]=O>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:7]([NH:9][C:10]2[C:11]([NH:16][C:17]([CH:19]3[CH2:20][CH2:21][N:22]([CH2:30][C:29]4[CH:32]=[CH:33][C:34]([OH:36])=[CH:35][C:28]=4[Cl:27])[CH2:23][CH2:24]3)=[O:18])=[CH:12][CH:13]=[CH:14][CH:15]=2)=[O:8])=[CH:25][CH:26]=1

참가 물질

반응물 2

HCID 1853632-Chloro-4-hydroxybenzaldehyde

HCID 53635745HCID 53635745, 화합물

생성물 1

HCID 21352696HCID 21352696, 화합물

실험 절차

Using the general procedure described in Example 3, N1-(4-methoxybenzoyl)-N2-(piperidin-4-ylcarbonyl)-1,2-benzenediamine (0.045 mmol) was reacted with 2-chloro-4-hydroxybenzaldehyde to provide 22 mg of the title product as the free base. Treatment with hydrochloric acid and concentration in vacuo yielded the salt of the title compound.

출처 및 근거

ORD 기록: ord-c5575f3b9f004d21bb000e49e14b0556
출처 데이터셋: uspto-grants-2003_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06605626B2

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