HCID 385601, 화합물 → HCID 18174628, 화합물

HRID 395753노트

반응식

HRID 395753 반응식
C(O[C:9]([NH:11][C:12]1[CH:13]=[C:14]([CH:16]=[CH:17][CH:18]=1)[NH2:15])=[O:10])C1C=CC=CC=1.[C:19]([C:23]1[CH:28]=[CH:27][C:26]([C:29]2[O:34]C(=O)[C:32]3[CH:36]=[CH:37][CH:38]=[CH:39][C:31]=3[N:30]=2)=[CH:25][CH:24]=1)([CH3:22])([CH3:21])[CH3:20]>>[NH2:15][C:14]1[CH:13]=[C:12]([NH:11][C:9](=[O:10])[C:32]2[CH:36]=[CH:37][CH:38]=[CH:39][C:31]=2[NH:30][C:29](=[O:34])[C:26]2[CH:25]=[CH:24][C:23]([C:19]([CH3:21])([CH3:20])[CH3:22])=[CH:28][CH:27]=2)[CH:18]=[CH:17][CH:16]=1

참가 물질

3

반응물 2

HCID 385601HCID 385601, 화합물HCID 12941491(3-Amino-phenyl)-carbamic acid benzyl ester

생성물 1

HCID 18174628HCID 18174628, 화합물수율 9%

실험 절차

By methods substantially equivalent to those described in Example 96, the title compound (40 mg, 9% for two steps) was prepared from m-(benzyloxycarbonylamino)aniline 1.5 mmol) and 2-(4-tert-butylphenyl)-4H-3,1-benzoxazin-4-one (1.5 mmol).

출처 및 근거

ORD 기록
ord-0d4269360b94417d87828f276f717309
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06605626B2

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