3-Benzyloxyaniline → 2-Amino-n-(3-benzyloxyphenyl)-4-nitrobenzamide

HRID 395764

반응식

[CH2:1]([O:8][C:9]1[CH:10]=[C:11]([CH:13]=[CH:14][CH:15]=1)[NH2:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N+:16]([C:19]1[CH:20]=[C:21]2[NH:27]C(=O)O[C:23](=[O:24])[C:22]2=[CH:29][CH:30]=1)([O-:18])=[O:17]>>[NH2:27][C:21]1[CH:20]=[C:19]([N+:16]([O-:18])=[O:17])[CH:30]=[CH:29][C:22]=1[C:23]([NH:12][C:11]1[CH:13]=[CH:14][CH:15]=[C:9]([O:8][CH2:1][C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)[CH:10]=1)=[O:24]

참가 물질

반응물 2

HCID 928923-Benzyloxyaniline

HCID 2820894-Nitro-isatoic anhydride

생성물 1

HCID 181745112-Amino-n-(3-benzyloxyphenyl)-4-nitrobenzamide수율 81%

실험 절차

Using the procedure described in Example 91, Part B, 3-benzyloxyaniline (4.4 mmol) and 4-nitroisatoic anhydride (4.8 mmol) yielded 1.2 g (81%) of the title product.

출처 및 근거

ORD 기록: ord-6bfbe3bb07cc4bca9bc0a354fbde3d3c
출처 데이터셋: uspto-grants-2003_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06605626B2

연결된 노트

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