4-Methylbenzoyl Chloride → N1-(4-Methylphenyl)-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine

HRID 395770노트

반응식

HRID 395770 반응식
[C:1]1([CH3:10])[CH:6]=[CH:5][C:4](C(Cl)=O)=[CH:3][CH:2]=1.[C:11]([C:15]1[CH:30]=[CH:29][C:18]([C:19]([NH:21][C:22]2[C:23]([NH2:28])=[CH:24][CH:25]=[CH:26][CH:27]=2)=[O:20])=[CH:17][CH:16]=1)([CH3:14])([CH3:13])[CH3:12]>>[CH3:10][C:1]1[CH:6]=[CH:5][C:4]([NH:28][C:23]2[C:22]([NH:21][C:19](=[O:20])[C:18]3[CH:29]=[CH:30][C:15]([C:11]([CH3:14])([CH3:12])[CH3:13])=[CH:16][CH:17]=3)=[CH:27][CH:26]=[CH:25][CH:24]=2)=[CH:3][CH:2]=1

참가 물질

3

반응물 2

HCID 134054-Methylbenzoyl ChlorideHCID 1133079N-(2-aminophenyl)-4-tert-butylbenzamide

생성물 1

HCID 57162673N1-(4-Methylphenyl)-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine수율 108%

실험 절차

Using the procedure described in Example 93, Part A, 4-toluoyl chloride (1.1 mmol) and N1-(4-tert-butylbenzoyl)-1,2-benzenediamine (0.93 mmol) yielded 360 mg (100%) of the title compound.

출처 및 근거

ORD 기록
ord-e107c204cc534fe3aca9acf84353ad80
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06605626B2

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