3-Methoxybenzoic Acid → N1-(3-Methoxybenzoyl)-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine

HRID 395771노트

반응식

HRID 395771 반응식
[C:1]([OH:11])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([O:8][CH3:9])[CH:3]=1.[C:12]([C:16]1[CH:31]=[CH:30][C:19]([C:20]([NH:22][C:23]2[C:24]([NH2:29])=[CH:25][CH:26]=[CH:27][CH:28]=2)=[O:21])=[CH:18][CH:17]=1)([CH3:15])([CH3:14])[CH3:13]>>[CH3:9][O:8][C:4]1[CH:3]=[C:2]([CH:7]=[CH:6][CH:5]=1)[C:1]([NH:29][C:24]1[C:23]([NH:22][C:20](=[O:21])[C:19]2[CH:30]=[CH:31][C:16]([C:12]([CH3:14])([CH3:13])[CH3:15])=[CH:17][CH:18]=2)=[CH:28][CH:27]=[CH:26][CH:25]=1)=[O:11]

참가 물질

3

반응물 2

HCID 114613-Methoxybenzoic AcidHCID 1133079N-(2-aminophenyl)-4-tert-butylbenzamide

생성물 1

HCID 10739879N1-(3-Methoxybenzoyl)-N2-(4-tert-butylbenzoyl)-1,2-benzenediamine수율 84.2%

실험 절차

Using the procedure described in Example 102, Part A, 3-anisic acid (3.6 mmol) and N1-(4-tert-butylbenzoyl)-1,2-benzenediamine (1.8 mmol) yielded 610 mg (84%) of the title compound.

출처 및 근거

ORD 기록
ord-bd8992a4fd1f4b08bbbd12ee97e43ce5
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06605626B2

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