4-Nitrobenzoic Acid → n1-(4-Nitrobenzoyl)-n2-(4-tert-butylbenzoyl)-1,2-benzenediamine

HRID 395773노트

반응식

HRID 395773 반응식
[C:1]([C:5]1[CH:20]=[CH:19][C:8]([C:9]([NH:11][C:12]2[C:13]([NH2:18])=[CH:14][CH:15]=[CH:16][CH:17]=2)=[O:10])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[N+:21]([C:24]1[CH:32]=[CH:31][C:27]([C:28](O)=[O:29])=[CH:26][CH:25]=1)([O-:23])=[O:22]>>[N+:21]([C:24]1[CH:25]=[CH:26][C:27]([C:28]([NH:18][C:13]2[C:12]([NH:11][C:9](=[O:10])[C:8]3[CH:19]=[CH:20][C:5]([C:1]([CH3:4])([CH3:2])[CH3:3])=[CH:6][CH:7]=3)=[CH:17][CH:16]=[CH:15][CH:14]=2)=[O:29])=[CH:31][CH:32]=1)([O-:23])=[O:22]

참가 물질

3

반응물 2

HCID 61084-Nitrobenzoic AcidHCID 1133079N-(2-aminophenyl)-4-tert-butylbenzamide

생성물 1

HCID 37699550n1-(4-Nitrobenzoyl)-n2-(4-tert-butylbenzoyl)-1,2-benzenediamine

실험 절차

Using the procedure described in Example 102, Part A, N1-(4-tert-butylbenzoyl)-1,2-benzenediamine (3.1 mmol) and 4-nitrobenzoic acid (3.0 mmol) yielded the title product, which was used directly in the next step without additional purification.

출처 및 근거

ORD 기록
ord-13e51588a921462394d334d966cf54d4
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06605626B2

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