3-Benzyloxyaniline → 2-[(4-Tert-butylbenzoyl)amino]-n-(3-benzyloxyphenyl)-5-nitrobenzamide

HRID 395786

반응식

HRID 395786 반응식
[CH2:1]([O:8][C:9]1[CH:10]=[C:11]([CH:13]=[CH:14][CH:15]=1)[NH2:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:16]([C:20]1[CH:25]=[CH:24][C:23]([C:26]2[O:31][C:30](=[O:32])[C:29]3[CH:33]=[C:34]([N+:37]([O-:39])=[O:38])[CH:35]=[CH:36][C:28]=3[N:27]=2)=[CH:22][CH:21]=1)([CH3:19])([CH3:18])[CH3:17]>>[C:16]([C:20]1[CH:25]=[CH:24][C:23]([C:26]([NH:27][C:28]2[CH:36]=[CH:35][C:34]([N+:37]([O-:39])=[O:38])=[CH:33][C:29]=2[C:30]([NH:12][C:11]2[CH:13]=[CH:14][CH:15]=[C:9]([O:8][CH2:1][C:2]3[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=3)[CH:10]=2)=[O:32])=[O:31])=[CH:22][CH:21]=1)([CH3:19])([CH3:17])[CH3:18]

참가 물질

3

반응물 2

HCID 928923-BenzyloxyanilineHCID 3855992-(4-Tert-butylphenyl)-6-nitro-3,1-benzoxazin-4-one

생성물 1

HCID 181744702-[(4-Tert-butylbenzoyl)amino]-n-(3-benzyloxyphenyl)-5-nitrobenzamide수율 42%

실험 절차

Using the procedure described in Example 91, Part B, 3-benzyloxyaniline (2.5 mmol) and 2-(4-tert-butylphenyl)-6-nitro-4H-3,1-benzoxazin-4-one (2.8 mmol) yielded 550 mg (42%) of the title compound.

출처 및 근거

ORD 기록
ord-4ae91a49d59f4d7ca3194e0b05198f68
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06605626B2

연결된 노트

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