Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → Ethanone, 1-(4-octylphenyl)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | Octylbenzene | HCID 16607 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | 1,1-Dichloroethane | HCID 6365 | — |
| 생성물 | Ethanone, 1-(4-octylphenyl)- | HCID 66344 | — |
반응 단계
Aluminum chloride (22.6 g) is suspended in dichloroethane (500 ml) and octylbenzene (16) (21.5 g) is added at room temperature. To the mixture is added acetyl chloride (8.87 g) under ice-cooling. The mixture is stirred at room temperature overnight. The reaction mixture is poured into ice water and extracted with ether. The organic layer is washed with brine and dried over sodium sulfate. The solvent is evaporated to give 4′-octylacetophenone (18′) as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06605744B2 |
| 출처 데이터셋 | uspto-grants-2003_08 |
| ORD ID | ord-f0335febdb6e4fc9a41e2e6dafd45797 |
| 출처 메모 | uspto-grants-2003_08 |