Sodium Sulfite → Sodium cycloheptylmethanesulfonate

HRID 397684노트

반응식

HRID 397684 반응식
Br[CH2:2][CH:3]1[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.[S:10]([O-:13])([O-:12])=[O:11].[Na+:14].[Na+]>>[CH:3]1([CH2:2][S:10]([O-:13])(=[O:12])=[O:11])[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.[Na+:14]

참가 물질

3

반응물 2

HCID 24437Sodium SulfiteHCID 23000753(Bromomethyl)cycloheptane

생성물 1

HCID 23670189Sodium cycloheptylmethanesulfonate

실험 절차

The subtitle compound was prepared by the method of Preparation 61 from 1-(bromomethyl)cycloheptane [Preparation 66] and sodium sulfite. The crude product was purified by recrystallisation from water to afford sodium cycloheptylmethanesulfonate as a white solid.

후처리

  1. customThe crude product was purified by recrystallisation from water

출처 및 근거

ORD 기록
ord-492a299d80e24777a8278b20b341f235
출처 데이터셋
uspto-grants-2003_08
특허 번호
US06610707B1

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