Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenol → Di-tert-butyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenol | HCID 996 | — |
| 반응물 | Ethyl acetate hexane | HCID 21226206 | — |
| 반응물 | N,N'-dimethyl-O-t-butylisourea | HCID 23001675 | — |
| 생성물 | Di-tert-butyl ether | HCID 22541 | 15% |
반응 단계
Following a procedure analogous to (3b), the phenol from (3a) (270 mg, 0.97 mmol) was reacted with N,N′-dimethyl-O-t-butylisourea. Silica gel chromatography (ethyl acetate-hexane, 20:80) gave the t-butyl ether (50.2 mg, 15%) as a 1:1 mixture of two isomers. MS found: (M+H)+=334.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06610731B2 |
| 출처 데이터셋 | uspto-grants-2003_08 |
| ORD ID | ord-06a1d31e4388451ab0e3ab6eef91a634 |
| 출처 메모 | uspto-grants-2003_08 |