Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Hexanol → N1-(1-Methylethyl)-1,4-benzenediamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Hexanol | HCID 8103 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | N-isopropyl-4-nitrosoaniline | HCID 21909787 | — |
| 생성물 | N1-(1-Methylethyl)-1,4-benzenediamine | HCID 85306 | — |
반응 단계
Following essentially the procedure of Example 1, 66.0 g (0.25 mole) N-isopropyl-4-nitrosoaniline, 20 g (50%) sodium hydroxide and 264 g n-hexanol were kept at 100° C. for 1.5 hours. HPLC analysis of the reaction mixture indicated absence of the nitroso starting compound. By vacuum distillation (95°-101° C. at 13.3-26.6 Pa), 31.3 g of product were recovered (48.6 wt. % yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04723040 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-c383faf3f6174cd6aefc2d5b32c406fe |
| 출처 메모 | uspto-grants-1988_02 |