Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
{[4-(Methylsulfanyl)phenyl]methyl}(triphenyl)phosphanium chloride → HCID 12652959, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | {[4-(Methylsulfanyl)phenyl]methyl}(triphenyl)phosphanium chloride | HCID 18969794 | — |
| 촉매 | Benzyltriphenylphosphonium chloride | HCID 70671 | — |
| 생성물 | HCID 12652959 | HCID 12652959 | — |
반응 단계
Following the procedure as describe in method 1, but sustituting 4-methylthiobenzyltriphenylphosphonium chloride for benzyltriphenylphosphonium chloride, the desired residue was purified by flash chromatography (silica gel; hexane/EtOAc (90:10)) and recrystallisation from hexane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05817700 |
| 출처 데이터셋 | uspto-grants-1998_10 |
| ORD ID | ord-92dd2f6185b44d6eb92558a7134d09c5 |
| 출처 메모 | uspto-grants-1998_10 |